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PubMed Publications| Keyword search (4,163 papers available) |  |
"J Anal Toxicol" Category Publications:
| Title | Authors | PubMed ID | |
|---|---|---|---|
| 1 | Enzymatic assay for GHB determination in forensic matrices. | Grenier V, Huppé G, Lamarche M, Mireault P | 22722059 MASSSPEC |
| 2 | Procedure for the Selection and Validation of a Calibration Model I-Description and Application | Brigitte Desharnais | 28137730 CHEMBIOCHEM |
| 3 | Procedure for the Selection and Validation of a Calibration Model II-Theoretical Basis | Brigitte Desharnais | 28158619 CHEMBIOCHEM |
| 4 | Challenges Related to Three Cases of Fatal Intoxication to Multiple Novel Synthetic Opioids. | Garneau B, Desharnais B, Beauchamp-Doré A, Lavallée C, Mireault P, Lajeunesse A | 30927001 CHEMBIOCHEM |
| 5 | A Tool for Automatic Correction of Endogenous Concentrations: Application to BHB Analysis by LC-MS-MS and GC-MS | Desharnais B; Lajoie MJ; Laquerre J; Savard S; Mireault P; Skinner CD; | 31141151 CHEMBIOCHEM |
| Title: | Procedure for the Selection and Validation of a Calibration Model II-Theoretical Basis | ||||
| Authors: | Brigitte Desharnais | ||||
| Link: | https://pubmed.ncbi.nlm.nih.gov/28158619/ | ||||
| Publication: | Journal of analytical toxicology | ||||
| Keywords: | |||||
| PMID: | 28158619 | Category: | J Anal Toxicol | Date Added: | 2019-05-31 |
| Dept Affiliation: |
CHEMBIOCHEM
1 Laboratoire de sciences judiciaires et de médecine légale, Department of Toxicology, 1701 rue Parthenais, Montréal, Québec, Canada H2K 3S7. 2 Department of Chemistry and Biochemistry, Concordia University, 7141 Sherbrooke Street West, Montréal, Québec, Canada H4B 1R6. 3 Department of Mathematics, Université de Sherbrooke, 2500 boulevard de l'Université, Sherbrooke, Québec, CanadaJ1K 2R1. 4 Laboratoire de sciences judiciaires et de médecine légale, Department of Toxicology, 1701 rue Parthenais, Montréal, Québec, CanadaH2K 3S7. 5 Department of Chemistry and Biochemistry, Concordia University, 7141 Sherbrooke Street West, Montréal, Québec, CanadaH4B 1R6. |
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Description: |
In the first part of this paper (I-Description and application), an automated, stepwise and analyst-independent process for the selection and validation of calibration models was put forward and applied to two model analytes. This second part presents the mathematical reasoning and experimental work underlying the selection of the different components of this procedure. Different replicate analysis designs (intra/inter-day and intra/inter-extraction) were tested and their impact on test results... |
